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of the screw at the end of the shot indicates a leaking check
valve. A leaking check valve will prevent a cushion from being
maintained and can cause random short shots and shot-to-shot
variability.
Back pressure
Typical back pressure is 7–10 bar (100–150 psi), though it may be
as low as 3.5 bar (50 psi). To improve melt uniformity, increase
melt temperature, or eliminate air entrapment (air splay),
back pressure can be increased to as much as 28 bar (400 psi).
Excessively high back pressures can aggravate drooling into the
mold since decompression is usually kept to a minimum.
Decompression
In general, minimal decompression is used. Decompression
tends to pull air back into the nozzle, causing splay in the next
shot. Small amounts of decompression can be used to reduce drool.
Trial preparation and operation
Before beginning a trial, be sure that all conditions are optimized.
• Check the dryer for proper:
– Air temperature at the hopper entrance
– Dew point of the drying air
– Airflow
– Hopper capacity relative to the size of sample to be dried
• Clean the hopper and material-handling system thoroughly.
• Ensure proper mold temperature control is available.
• Check the chiller and thermolator.
• Be sure the molding machine is clean. (See the section on
start-up and purging.)
• Determine trial objectives. The purpose of the trial dictates
the amount of material needed and the quality and number of
parts required. For example, if the purpose is to obtain 5 good
parts for testing, it is typical to run 200 shots on an untried
mold. If the purpose is to make 50 parts, minimize cycle,
or check part variability, the amount of material and time
required will be much greater.
It is important to keep a complete record of operating conditions,
pretrial preparations, changes, etc. during the trial. Forms for
documenting trial procedures are provided for your convenience.
Completing Form 1 (“Pretrial preparation,” page 41) helps ensure
that all needed preliminary operations have been performed.
Form 2 (“Molding conditions record,” page 42) and Form 3
(“Identifying problems that are causing scrap,” page 43) can
be used during the molding trial. Changes made to processing
variables and effects of those changes during the trial or
start-up can be documented on Form 3.
• Retain 30- to 60-g (1- to 2-oz) samples of the pellets and
parts for follow-up testing of Ih.V. (inherent viscosity) or
molecular weight.
• Document and save all setup conditions, changes to conditions,
and their effects on part quality. Add comments regarding
what worked well and what caused problems. Provide copies
to all trial team members and to your Eastman representative.
When the job goes to production, give copies to all persons
involved.
Start-up
Start with a clean machine. If the machine is not purged,
unmelted particles, gaseous splay, or a combination of problems
will result. Ball checks are typically slow to purge and generally
are not recommended; check rings are preferred.
Removing and cleaning the screw, check valve, nozzle, and barrel
are the only effective means of purging difficult-to-remove
high-temperature plastics.
Purge materials
The material most effective in purging is a polymer similar to
the material to be run. Polyethylene and polypropylene should
be avoided because they can mix with the new material and
cause streaks for extended periods of time. For difficult-to-
remove materials, nozzle and front barrel zone setpoints are
sometimes increased up to 300°C (570°F) to soak and purge,
then cooled back to running temperatures. Use caution and
refer to the manufacturer’s recommendations for the material
used in the previous run.
After any cycle interruption of more than approximately 5
minutes, purging 3–5 shots is good practice.
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